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In Situ Solid–Gas Reactivity of Nanoscaled Metal Borides from Molten Salt Synthesis

Abstract : The reactivity of metal boride nanocrystals versus reducing and oxidizing atmospheres at 400 °C is probed by in situ electron microscopy and near-ambient pressure X-ray photoelectron and near-edge X-ray absorption spectroscopies. This combination unveils a decomposition process of the borides and sheds light on the strong dependency of their stability on the nature of the surrounding medium.
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https://hal.sorbonne-universite.fr/hal-01739853
Contributor : Isabelle Vuillaume <>
Submitted on : Wednesday, March 21, 2018 - 2:13:54 PM
Last modification on : Wednesday, September 23, 2020 - 4:35:18 AM

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Guillaume Gouget, Damien Debecker, Ara Kim, Giorgia Olivieri, Jean-Jacques Gallet, et al.. In Situ Solid–Gas Reactivity of Nanoscaled Metal Borides from Molten Salt Synthesis. Inorganic Chemistry, American Chemical Society, 2017, 56 (15), pp.9225 - 9234. ⟨10.1021/acs.inorgchem.7b01279⟩. ⟨hal-01739853⟩

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