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Morphological control of ZnS nanopowders by different capping molecules

Anael Jaffres 1 Damien Bregiroux 1 David Reekie 2 Robert Shears 2
1 MHN - Matériaux Hybrides et Nanomatériaux
LCMCP - Laboratoire de Chimie de la Matière Condensée de Paris
Abstract : Complex 3D architectures of ZnS microflowers have been successfully synthesized via a quick water-based precipitation synthesis method at moderate temperature (<100°C) using an inorganic capping agent K 2 S 2 O 7. The synthesized samples were characterized by SEM, XRD, FTIR and BET analysis. The as-synthesized ZnS microflowers are composed of numerous nanowires and has a cubic structure. Surface area is 42 m 2 .g-1 and the pore diameter is 3.7 nm. Comparison with equivalent synthesis with an organic capping agent (PVP) was performed.
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Submitted on : Friday, December 1, 2017 - 1:47:17 PM
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Anael Jaffres, Damien Bregiroux, David Reekie, Robert Shears. Morphological control of ZnS nanopowders by different capping molecules. Materials Letters, Elsevier, 2017, 209, pp.539-542. ⟨10.1016/j.matlet.2017.08.102⟩. ⟨hal-01653385⟩

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